Purification, crystallization and preliminary crystallographic study of a Kunitz-type trypsin inhibitor from Delonix regia seeds

Acta Crystallogr D Biol Crystallogr. 1999 Sep;55(Pt 9):1611-3. doi: 10.1107/s0907444999009361.

Abstract

The Kunitz-type trypsin inhibitor from seeds of Flamboyant (Delonix regia) has been purified to homogeneity and plate-like crystals suitable for X-ray analysis have been grown by the hanging-drop method using PEG 6000 as a precipitant. The crystals belong to space group P2(1)2(1)2(1) with unit-cell parameters a = 32.15, b = 69.39, c = 72.54 A. X-ray diffraction data have been collected to 2.95 A resolution. The structure has been solved by molecular replacement using the known structures of trypsin inhibitors from Erythrina caffra seeds (PDB code 1tie) and from soya beans (Glycine max; PDB code 1ba7) as search models.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Crystallization
  • Crystallography, X-Ray
  • Seeds / chemistry*
  • Trees
  • Trypsin Inhibitor, Kunitz Soybean / chemistry*
  • Trypsin Inhibitor, Kunitz Soybean / isolation & purification

Substances

  • Trypsin Inhibitor, Kunitz Soybean