Inversion of in situ synthesized oligonucleotides: improved reagents for hybridization and primer extension in DNA microarrays

Nucleic Acids Res. 1999 Dec 15;27(24):4710-4. doi: 10.1093/nar/27.24.4710.

Abstract

Oligonucleotides synthesized in array format suffer from contamination by truncated species. We have developed a method to invert DNA molecules in situ after completed synthesis. Reactive functions at the 5'-ends of the oligonucleotides are permitted to react with functions on the support before the 3'-ends are released, in effect reversing the orientation of full-length oligonucleotides, while any 5'-truncated molecules are lost. This strategy serves both to purify in situ synthesized reagents and to reorient the oligonucleotides, causing them to expose free 3'-hydroxyls. In situ inverted oligonucleotides can be used in assays based on DNA polymerase-assisted extension of immobilized primers, and we demonstrate their utility in minisequencing and in pyrosequencing.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Base Sequence
  • DNA Primers / chemical synthesis
  • DNA Primers / chemistry*
  • Indicators and Reagents
  • Nucleic Acid Hybridization / methods*
  • Oligodeoxyribonucleotides / chemical synthesis*
  • Oligodeoxyribonucleotides / chemistry*
  • Oligonucleotide Array Sequence Analysis*

Substances

  • DNA Primers
  • Indicators and Reagents
  • Oligodeoxyribonucleotides