Abstract
Investigation of the hooks of Uncaria rhynchophylla resulted in isolation of six phospholipase Cgamma1 (PLCgamma1) inhibitors (1-6). The structures of these compounds were elucidated as pentacyclic triterpene esters by spectroscopic and chemical analysis. Three of them, namely uncarinic acids C (1), D (2), and E (3), are newly reported as natural products. All the compounds showed dose-dependent inhibitory activities against PLCgamma1 in vitro with IC(50) values of 9.5-44.6 microM and inhibited the proliferation of human cancer cells with IC(50) values of 0.5-6.5 microg/mL.
Publication types
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Research Support, Non-U.S. Gov't
MeSH terms
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3T3 Cells
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Animals
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Cell Division / drug effects
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Dose-Response Relationship, Drug
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Enzyme Inhibitors / isolation & purification*
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Enzyme Inhibitors / pharmacology
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Esters / isolation & purification*
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Esters / pharmacology*
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Humans
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Isoenzymes / antagonists & inhibitors*
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Mice
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Neoplasms / enzymology
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Neoplasms / pathology*
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Phospholipase C gamma
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Plants, Medicinal / chemistry*
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Rubiaceae / chemistry*
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Structure-Activity Relationship
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Triterpenes / isolation & purification*
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Triterpenes / pharmacology*
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Tumor Cells, Cultured
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Type C Phospholipases / antagonists & inhibitors*
Substances
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Enzyme Inhibitors
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Esters
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Isoenzymes
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Triterpenes
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uncarinic acid-C
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uncarinic acid-D
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uncarinic acid-E
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Type C Phospholipases
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Phospholipase C gamma