Novel histamine H(3)-receptor antagonists and partial agonists with a non-aminergic structure

Br J Pharmacol. 2001 Apr;132(8):1665-72. doi: 10.1038/sj.bjp.0704013.

Abstract

We determined the affinities of eight novel histamine H(3)-receptor ligands (ethers and carbamates) for H(3)-receptor binding sites and their agonistic/antagonistic effects in two functional H(3)-receptor models. The compounds differ from histamine in that the ethylamine chain is replaced by a propyloxy chain; in the three ethers mentioned below (FUB 335, 373 and 407), R is n-pentyl, 3-methylbutyl and 3,3-dimethylbutyl, respectively. The compounds monophasically inhibited [(3)H]-N(alpha)-methylhistamine binding to mouse cerebral cortex membranes (pK(i) 7.51 - 9.53). The concentration-response curve of histamine for its inhibitory effect on the electrically evoked [(3)H]-noradrenaline overflow from mouse cortex slices was shifted to the right by these compounds (apparent pA(2) 6.61 - 8.00). Only FUB 373 and 407 inhibited the evoked overflow by themselves (intrinsic activities 0.3 and 0.4); these effects were counteracted by the H(3)-receptor antagonist clobenpropit. [(35)S]-GTPgammaS binding to mouse cortex membranes was stimulated by the H(3)-receptor agonist (R)-alpha-methylhistamine in a manner sensitive to clobenpropit. Among the novel compounds only FUB 373 and 407 stimulated [(35)S]-GTPgammaS binding (intrinsic activities 0.6 and 0.4). In conclusion, the novel compounds are partial H(3)-receptor agonists (FUB 373 and 407) or H(3)-receptor antagonists; comparison with FUB 335 shows that the transition from antagonist to agonist is caused by a slight structural change. A protonated N atom in the side chain is not necessary for agonism at H(3) receptors, proposing a receptor-ligand interaction different from that of classical agonists.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amines / chemistry
  • Animals
  • Brain Chemistry / drug effects
  • Cerebral Cortex / drug effects
  • Cerebral Cortex / metabolism
  • Electric Stimulation
  • Guanosine 5'-O-(3-Thiotriphosphate) / metabolism
  • Histamine / pharmacology
  • Histamine Agonists / chemistry
  • Histamine Agonists / pharmacology*
  • Histamine Antagonists / pharmacology*
  • In Vitro Techniques
  • Methylhistamines / pharmacology
  • Mice
  • Norepinephrine / metabolism
  • Perfusion
  • Rats
  • Rats, Wistar
  • Receptors, Histamine H3 / drug effects*

Substances

  • Amines
  • Histamine Agonists
  • Histamine Antagonists
  • Methylhistamines
  • Receptors, Histamine H3
  • Guanosine 5'-O-(3-Thiotriphosphate)
  • alpha-methylhistamine
  • Histamine
  • Norepinephrine