Catalytic domain structures of MT-SP1/matriptase, a matrix-degrading transmembrane serine proteinase

J Biol Chem. 2002 Jan 18;277(3):2160-8. doi: 10.1074/jbc.M109830200. Epub 2001 Nov 5.

Abstract

The type II transmembrane multidomain serine proteinase MT-SP1/matriptase is highly expressed in many human cancer-derived cell lines and has been implicated in extracellular matrix re-modeling, tumor growth, and metastasis. We have expressed the catalytic domain of MT-SP1 and solved the crystal structures of complexes with benzamidine at 1.3 A and bovine pancreatic trypsin inhibitor at 2.9 A. MT-SP1 exhibits a trypsin-like serine proteinase fold, featuring a unique nine-residue 60-insertion loop that influences interactions with protein substrates. The structure discloses a trypsin-like S1 pocket, a small hydrophobic S2 subsite, and an open negatively charged S4 cavity that favors the binding of basic P3/P4 residues. A complementary charge pattern on the surface opposite the active site cleft suggests a distinct docking of the preceding low density lipoprotein receptor class A domain. The benzamidine crystals possess a freely accessible active site and are hence well suited for soaking small molecules, facilitating the improvement of inhibitors. The crystal structure of the MT-SP1 complex with bovine pancreatic trypsin inhibitor serves as a model for hepatocyte growth factor activator inhibitor 1, the physiological inhibitor of MT-SP1, and suggests determinants for the substrate specificity.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Base Sequence
  • Binding Sites
  • Catalytic Domain
  • Crystallography, X-Ray
  • DNA Primers
  • Extracellular Matrix / metabolism*
  • Humans
  • Hydrolysis
  • Models, Molecular
  • Molecular Sequence Data
  • Protein Conformation
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / metabolism
  • Sequence Homology, Amino Acid
  • Serine Endopeptidases / chemistry
  • Serine Endopeptidases / metabolism*
  • Substrate Specificity
  • Trypsin / chemistry
  • Trypsin / metabolism*
  • Tumor Cells, Cultured

Substances

  • DNA Primers
  • Recombinant Proteins
  • Serine Endopeptidases
  • matriptase
  • ST14 protein, human
  • Trypsin

Associated data

  • PDB/1EAW
  • PDB/1EAX