Cellular solid-phase binding assay and mass spectrometry for screening of alpha 4 beta 7 integrin antagonists

Bioorg Med Chem Lett. 2001 Dec 3;11(23):2997-3000. doi: 10.1016/s0960-894x(01)00611-4.

Abstract

A qualitative cellular solid-phase binding assay for screening alpha 4 beta 7 integrin antagonists attached via photolinker to TentaGel Macrobeads has been developed. An activation of the integrins with Mn(2+) was necessary to achieve binding to the bead bound antagonists. The identification of the resin bound compounds was done by mass spectrometry.

MeSH terms

  • Cell Adhesion
  • Drug Evaluation, Preclinical / methods*
  • Humans
  • Integrins / antagonists & inhibitors*
  • Integrins / metabolism*
  • Mass Spectrometry / methods*
  • Tumor Cells, Cultured

Substances

  • Integrins
  • integrin alpha4beta7