HIV-1 integrase forms stable tetramers and associates with LEDGF/p75 protein in human cells

J Biol Chem. 2003 Jan 3;278(1):372-81. doi: 10.1074/jbc.M209278200. Epub 2002 Oct 28.

Abstract

We studied human immunodeficiency virus, type 1 (HIV-1) integrase (IN) complexes derived from nuclei of human cells stably expressing the viral protein from a synthetic gene. We show that in the nuclear extracts IN exists as part of a large distinct complex with an apparent Stokes radius of 61 A, which dissociates upon dilution yielding a core molecule of 41 A. We isolated the IN complexes from cells expressing FLAG-tagged IN and demonstrated that the 41 A core is a tetramer of IN, whereas 61 A molecules are composed of IN tetramers associated with a cellular protein with an apparent molecular mass of 76 kDa. This novel integrase interacting protein was found to be identical to lens epithelium-derived growth factor (LEDGF/p75), a protein implicated in regulation of gene expression and cellular stress response. HIV-1 IN and LEDGF co-localized in the nuclei of human cells stably expressing IN. Furthermore, recombinant LEDGF robustly enhanced strand transfer activity of HIV-1 IN in vitro. Our findings indicate that the minimal IN molecule in human cells is a homotetramer, suggesting that at least an octamer of IN is required to accomplish coordinated integration of both retroviral long terminal repeats and that LEDGF is a cellular factor involved in this process.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Cell Fractionation
  • Cell Line
  • Cell Nucleus / metabolism
  • Cross-Linking Reagents / metabolism
  • HIV Integrase / chemistry
  • HIV Integrase / genetics
  • HIV Integrase / metabolism*
  • Humans
  • Intercellular Signaling Peptides and Proteins / chemistry
  • Intercellular Signaling Peptides and Proteins / genetics
  • Intercellular Signaling Peptides and Proteins / metabolism*
  • Macromolecular Substances
  • Molecular Sequence Data
  • Molecular Weight
  • Peptides / genetics
  • Peptides / metabolism
  • Protein Structure, Quaternary*
  • Recombinant Proteins / genetics
  • Recombinant Proteins / metabolism
  • Succinimides / metabolism
  • Virus Integration / physiology*

Substances

  • Cross-Linking Reagents
  • Intercellular Signaling Peptides and Proteins
  • Macromolecular Substances
  • Peptides
  • Recombinant Proteins
  • Succinimides
  • lens epithelium-derived growth factor
  • 3,3'-dithiobis(sulfosuccinimidyl propionate)
  • HIV Integrase