Abstract
We have developed concise and efficient syntheses of novel spirocyclic pyrrolidones 1-3, which involve the alkylation of pyrrolidone precursor 13 with 1,5-dibromopentane, 16 and 15, followed by an in situ lactamization. Conjugates of 1 and 2 with P1'/P2' hydroxy-indanolamine moiety resulted in novel and potent inhibitors of HIV-1 protease 25 and 26, suggesting that 1 and 2 are novel P2/P1 HIV-PI mimetics.
MeSH terms
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Alkylation
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Anti-HIV Agents / chemistry
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Anti-HIV Agents / pharmacology
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Biomimetic Materials / chemistry
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Biomimetic Materials / pharmacology
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HIV Protease Inhibitors / chemistry*
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HIV Protease Inhibitors / pharmacology*
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Lactams / chemistry
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Pyrrolidinones / chemistry*
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Pyrrolidinones / pharmacology*
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Spiro Compounds / chemistry
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Spiro Compounds / pharmacology
Substances
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Anti-HIV Agents
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HIV Protease Inhibitors
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Lactams
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Pyrrolidinones
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Spiro Compounds