Posttranslational modification of serine to formylglycine in bacterial sulfatases. Recognition of the modification motif by the iron-sulfur protein AtsB

J Biol Chem. 2003 Jan 24;278(4):2212-8. doi: 10.1074/jbc.M209435200. Epub 2002 Nov 4.

Abstract

Calpha-formylglycine is the catalytic residue of sulfatases. Formylglycine is generated by posttranslational modification of a cysteine (pro- and eukaryotes) or serine (prokaryotes) located in a conserved (C/S)XPXR motif. The modifying enzymes are unknown. AtsB, an iron-sulfur protein, is strictly required for modification of Ser(72) in the periplasmic sulfatase AtsA of Klebsiella pneumoniae. Here we show (i) that AtsB is a cytosolic protein acting on newly synthesized serine-type sulfatases, (ii) that AtsB-mediated FGly formation is dependent on AtsA's signal peptide, and (iii) that the cytosolic cysteine-type sulfatase of Pseudomonas aeruginosa can be converted into a substrate of AtsB if the cysteine is substituted by serine and a signal peptide is added. Thus, formylglycine formation in serine-type sulfatases depends both on AtsB and on the presence of a signal peptide, and AtsB can act on sulfatases of other species. AtsB physically interacts with AtsA in a Ser(72)-dependent manner, as shown in yeast two-hybrid and GST pull-down experiments. This strongly suggests that AtsB is the serine-modifying enzyme and that AtsB relies on a cytosolic function of the sulfatase's signal peptide.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alanine / analogs & derivatives*
  • Alanine / chemistry
  • Amino Acid Motifs
  • Amino Acid Sequence
  • Arylsulfatases / chemistry*
  • Arylsulfatases / metabolism
  • Blotting, Western
  • Cysteine / metabolism
  • Cytosol / metabolism
  • Dose-Response Relationship, Drug
  • Escherichia coli / metabolism
  • Glutathione Transferase / metabolism
  • Glycine / analogs & derivatives*
  • Glycine / chemistry*
  • Iron-Sulfur Proteins / chemistry*
  • Iron-Sulfur Proteins / metabolism
  • Klebsiella pneumoniae / metabolism
  • Models, Chemical
  • Molecular Sequence Data
  • Mutagenesis, Site-Directed
  • Peptides / chemistry
  • Protein Binding
  • Protein Processing, Post-Translational*
  • Protein Sorting Signals
  • Serine / chemistry*
  • Serine / metabolism
  • Subcellular Fractions
  • Sulfatases / metabolism*
  • Two-Hybrid System Techniques
  • beta-Galactosidase / metabolism

Substances

  • AtsA protein, Klebsiella pneumoniae
  • AtsB protein, Klebsiella pneumoniae
  • Iron-Sulfur Proteins
  • Peptides
  • Protein Sorting Signals
  • Serine
  • C(alpha)-formylglycine
  • Glutathione Transferase
  • Sulfatases
  • Arylsulfatases
  • beta-Galactosidase
  • Cysteine
  • Alanine
  • Glycine