[Methodological studies on quantitative determination of beta-eudesmol in Atractylodes lancea (thunb.) DC]

Zhongguo Zhong Yao Za Zhi. 2000 Nov;25(11):680-1.
[Article in Chinese]

Abstract

Objective: To establish methodologically a method for quantitative determination of beta-eudesmol in Atractylodes lancea.

Method: GC, column: 3 mm x 2 m; stationary phase; 15% QF-1; support: Chromosorb WAW(60-80 mesh); detector: hydrogen flame ionization detector; injection chamber temperature: 210 degrees C; column temperature: 174 degrees C; carrier gas: N2:50 ml.min-1, air: 49 kPa, H2:58.8 kPa; sensibility range: 10(2) x 64; chart speed: 2.5 mm.min-1.

Result: Average recovery ratio is 100.7% (n = 5).

Conclusion: This method can be used to control the quality of A. lancea.

Publication types

  • English Abstract

MeSH terms

  • Atractylodes / chemistry*
  • Chromatography, Gas
  • Drugs, Chinese Herbal / analysis
  • Plant Roots / chemistry
  • Plants, Medicinal / chemistry*
  • Quality Control
  • Sesquiterpenes, Eudesmane*
  • Terpenes / analysis*

Substances

  • Drugs, Chinese Herbal
  • Sesquiterpenes, Eudesmane
  • Terpenes
  • beta-eudesmol