Enhanced blood compatibility of polymers grafted by sulfonated PEO via a negative cilia concept

Biomaterials. 2003 Jun;24(13):2213-23. doi: 10.1016/s0142-9612(03)00023-1.

Abstract

In our laboratory sulfonated PEO (PEO-SO(3)) was designed as a "negative cilia model" to investigate a synergistic effect of PEO and negatively charged SO(3) groups. PEO-SO(3) itself exhibited a heparin-like anticoagulant activity of 14% of free heparin. Polyurethane grafted with PEO-SO(3) (PU-PEO-SO(3)) increased the albumin adsorption to a great extent but suppressed other proteins, while PU-PEO decreased the adsorption of all the proteins. The platelet adhesion was decreased on PU-PEO but least on PU-PEO-SO(3) to demonstrate an additional effect of SO(3) groups. The enhanced blood compatibility of PU-PEO-SO(3) in the ex vivo rabbit and in vivo canine implanting tests was confirmed. Furthermore, PU-PEO-SO(3) exhibited an improved biostability and suppressed calcification in addition to the enhanced antithrombogenicity. The in vivo antithrombogenicity and biostability were improved in the order of PU<PU-PEO<PU-PEO-SO(3). The calcium amounts deposited was decreased in the order of PU>PU-PEO>PU-PEO-SO(3) in spite of the possible attraction between negative SO(3) groups and positive calcium ions. The bioprosthetic tissue (BT) was grafted with H(2)N-PEO-SO(3) via glutaraldehyde (GA) residues after conventional GA fixation. BT-PEO-SO(3) also displayed the decreased calcification by in vivo animal models. The application of PEO-SO(3) was extended by designing amphiphilic copolymers containing PEO-SO(3) moiety and hydrophobic long alkyl groups as anchors. The superior effect of PEO-SO(3) groups on thromboresistance compared to PEO was confirmed also in the case of copolymers coated or blended with other polymers and the systems coupled by UV irradiation, photoreaction or gold/sulfur or silane coupling technology, and therefore it might be very useful for the medical devices.

Publication types

  • Comparative Study
  • Evaluation Study
  • Research Support, Non-U.S. Gov't
  • Validation Study

MeSH terms

  • Adsorption
  • Animals
  • Biocompatible Materials / chemical synthesis
  • Biocompatible Materials / chemistry*
  • Blood Coagulation / physiology*
  • Blood Physiological Phenomena
  • Blood Proteins / chemistry*
  • Histocompatibility*
  • Humans
  • Materials Testing
  • Platelet Activation / physiology
  • Polyethylene Glycols / chemistry*
  • Polymers / chemistry
  • Sulfonic Acids / chemistry*
  • Surface Properties
  • Thrombosis / prevention & control*
  • Tissue Engineering / instrumentation
  • Tissue Engineering / methods*
  • Transplants

Substances

  • Biocompatible Materials
  • Blood Proteins
  • Polymers
  • Sulfonic Acids
  • amino-polyethyleneoxide-sulfonate
  • Polyethylene Glycols