Isolation and partial characterization of a compound with siderophore activity from Vibrio parahaemolyticus

FEMS Microbiol Lett. 1992 Jul 1;73(1-2):181-6. doi: 10.1016/0378-1097(92)90605-n.

Abstract

A compound with siderophore activity was purified by successive column and thin layer chromatographic procedures from Dowex 1 x 8 extracts of culture supernatants of Vibrio parahaemolyticus AQ 3354. The strain synthesized the compound in culture media containing less than 2 microM added FeCl3. Hydrolysis of the compound yielded alanine, ethanolamine, citric acid and 2-ketoglutaric acid. The 1H-NMR spectrum exhibited the presence of a residue from each of these components in the intact molecule. The fast-atom bombardment mass spectrum of the methyl ester derivative indicated a prominent ion at m/z 477, probably corresponding to [M + 1] ion. Other strains of V. parahaemolyticus were also found to produce this compound when grown in an iron-limited medium.

MeSH terms

  • Cell Fractionation
  • Hydrolysis
  • Iron Chelating Agents / chemistry*
  • Iron Chelating Agents / isolation & purification
  • Iron Chelating Agents / metabolism
  • Siderophores
  • Species Specificity
  • Vibrio parahaemolyticus / chemistry*

Substances

  • Iron Chelating Agents
  • Siderophores