Synthesis of novel 6,11-O-bridged bicyclic ketolides via a palladium-catalyzed bis-allylation

Org Lett. 2004 Nov 25;6(24):4455-8. doi: 10.1021/ol048336r.

Abstract

A bridging chemistry process was developed to form an ether bridge between 6-O and 11-O of erythromycin A via a tandem or stepwise palladium-catalyzed bis-pi-allylation. By applying this bridging process, new 6,11-O-bridged bicyclic ketolides (BBKs) were synthesized. These BBKs showed good antibacterial activities against the macrolide-susceptible strains as well as mef-resistant strains and served as a good core for further modifications to study the structure-activity relationship (SAR) and to overcome bacterial resistance. [reaction: see text]