Synthesis of a novel conformationally restricted Val-Phe dipeptidomimetic

J Pept Sci. 2006 Feb;12(2):140-6. doi: 10.1002/psc.688.

Abstract

A method for the synthesis of (3(R,S),6S,11b(R,S))-1,3,4,6,7,11b-hexahydro-4-oxo-3-phthalimidopyrido[2,1-a]isoquinoline-6-carboxylic acid 2 as a new conformationally restricted dipeptidomimetic of Val-Phe is reported. It involved cyclisation via an intramolecular electrophilic addition at the reactive bridgehead carbon. This new scaffold can be used as a building block in the preparation of libraries of peptidomimetics.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Dipeptides / chemical synthesis*
  • Dipeptides / chemistry
  • Models, Molecular
  • Molecular Mimicry*
  • Nuclear Magnetic Resonance, Biomolecular
  • Phenylalanine / chemistry*
  • Protein Conformation
  • Valine / chemistry*

Substances

  • Dipeptides
  • Phenylalanine
  • Valine