Resonant soft X-ray diffraction - in extremis

J Synchrotron Radiat. 2005 Jul;12(Pt 4):434-41. doi: 10.1107/S0909049505009167. Epub 2005 Jun 15.

Abstract

The use of softer-energy X-rays produced by synchrotron radiation for diffraction is an area of current interest. In this paper, experiments exploiting resonant scattering at the L absorption edges of 3d transition metal elements are reported. Such energies, typically 500-1000 eV, are at the extreme limit of soft X-ray diffraction where absorption effects are so severe that the sample and diffractometer must be placed in a windowless high-vacuum vessel. In addition, the Ewald sphere is so small as to likely contain, at most, only a single Bragg reflection. Advantages of using such radiation for the study of weak diffraction effects such as anomalous scattering, charge ordering, magnetic diffraction and orbital ordering are reported.

Publication types

  • Research Support, Non-U.S. Gov't
  • Review

MeSH terms

  • Computer Simulation
  • Equipment Design
  • Magnetics / instrumentation*
  • Models, Chemical*
  • Molecular Conformation
  • X-Ray Diffraction / instrumentation*
  • X-Ray Diffraction / methods*
  • X-Ray Diffraction / trends