Identification and characterization of small molecule modulators of KChIP/Kv4 function

Bioorg Med Chem. 2005 Nov 15;13(22):6112-9. doi: 10.1016/j.bmc.2005.06.042. Epub 2005 Aug 2.

Abstract

Potassium channels and their associated subunits are important contributors to electrical excitability in many cell types. In this study, a yeast two-hybrid assay was used to identify inhibitors such as a diaryl-urea compound (CL-888) that binds to and modulates the formation of the Kv4/KChIP complex. CL-888 altered the apparent affinity of KChIP1 to Kv4.3-N in a Biacore assay, but did not dissociate the two proteins in size-exclusion chromatography experiments. Kv4.2/KChIP1 current amplitude and kinetics were altered with compound exposure, supporting the hypothesis of a compound-induced conformational change in the protein complex. Fluorescence spectroscopy of a unique tryptophan residue in KChIP1 was consistent with compound binding to the protein. Molecular modeling using the KChIP1 crystal structure indicates that compound binding may occur in a small tryptophan-containing binding pocket located on the hydrophilic side of the protein.

MeSH terms

  • Animals
  • Chromatography, Gel
  • Electrophysiology
  • Gene Transfer Techniques
  • Humans
  • Inhibitory Concentration 50
  • Kv Channel-Interacting Proteins / genetics
  • Kv Channel-Interacting Proteins / metabolism*
  • Models, Chemical
  • Models, Molecular
  • Oocytes / physiology
  • Protein Binding
  • Protein Conformation / drug effects
  • Shal Potassium Channels / genetics
  • Shal Potassium Channels / metabolism*
  • Spectrometry, Fluorescence
  • Two-Hybrid System Techniques
  • Urea / analogs & derivatives*
  • Urea / pharmacology
  • Xenopus

Substances

  • CL-888
  • Kv Channel-Interacting Proteins
  • Shal Potassium Channels
  • Urea