Recombinant human cathepsin X is a carboxymonopeptidase only: a comparison with cathepsins B and L

Biol Chem. 2005 Nov;386(11):1191-5. doi: 10.1515/BC.2005.136.

Abstract

The S1 and S2 subsite specificity of recombinant human cathepsins X was studied using fluorescence resonance energy transfer (FRET) peptides with the general sequences Abz-Phe-Xaa-Lys(Dnp)-OH and Abz-Xaa-Arg-Lys(Dnp)-OH, respectively (Abz=ortho-aminobenzoic acid and Dnp=2,4-dinitrophenyl; Xaa=various amino acids). Cathepsin X cleaved all substrates exclusively as a carboxymonopeptidase and exhibited broad specificity. For comparison, these peptides were also assayed with cathepsins B and L. Cathepsin L hydrolyzed the majority of them with similar or higher catalytic efficiency than cathepsin X, acting as an endopeptidase mimicking a carboxymonopeptidase (pseudo-carboxymonopeptidase). In contrast, cathepsin B exhibited poor catalytic efficiency with these substrates, acting as a carboxydipeptidase or an endopeptidase. The S1' subsite of cathepsin X was mapped with the peptide series Abz-Phe-Arg-Xaa-OH and the enzyme preferentially hydrolyzed substrates with hydrophobic residues in the P1' position.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Carboxypeptidases / chemistry*
  • Carboxypeptidases / genetics
  • Cathepsin B / chemistry*
  • Cathepsin B / genetics
  • Cathepsin K
  • Cathepsin L
  • Cathepsins / chemistry*
  • Cathepsins / genetics
  • Cysteine Endopeptidases / chemistry*
  • Cysteine Endopeptidases / genetics
  • Humans
  • Hydrolysis
  • Kinetics
  • Peptides / metabolism
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / genetics
  • Substrate Specificity / genetics
  • Substrate Specificity / physiology

Substances

  • Peptides
  • Recombinant Proteins
  • Carboxypeptidases
  • Cathepsins
  • Cysteine Endopeptidases
  • Cathepsin B
  • CTSL protein, human
  • Cathepsin L
  • CTSK protein, human
  • Cathepsin K