Measurement of total testosterone in women: comparison of a direct radioimmunoassay versus radioimmunoassay after organic solvent extraction and celite column partition chromatography

Fertil Steril. 2005 Dec;84(6):1698-704. doi: 10.1016/j.fertnstert.2005.05.058.

Abstract

Objective: To evaluate the clinical usefulness for the measurement of testosterone (T) values in the "low" female range with a direct radioimmunoassay (RIA) for total T by comparing total T values measured by this assay with values determined by conventional RIA after organic solvent extraction/column chromatography.

Design: Cross-sectional study.

Setting: Victoria, Australia.

Patient(s): Two hundred fifty-nine healthy women, aged 18-75 years, recruited from the community.

Intervention(s): Fasting serum samples were obtained and stored at -80 degrees C.

Main outcome measure(s): Total T measurement. Total T was measured by the direct RIA method using antibody-coated tubes and iodine-labeled T tracer. For comparison, total T levels were also measured using the conventional RIA method after organic solvent (ethyl acetate:hexane [3:2]) extraction and celite column partition chromatography before RIA.

Result(s): The mean T level by direct RIA was 0.76 nmol/L (median, 0.70; SD, 0.54; minimum, 0.10; maximum, 3.2). The mean difference between the two measurements (direct RIA - conventional RIA) was -0.28 (SD, 0.3). The direct RIA value was 63% (95% confidence interval, 26%-155%) of the conventional RIA estimate. For the classification of values at the lower end of the range, there was very good agreement beyond chance (kappa = 0.68-0.74) for values in approximately the lowest 10th-40th percentiles.

Conclusion(s): The direct RIA is a clinically useful assay for the study of the issue of "low" T within the female population.

Publication types

  • Clinical Trial
  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adolescent
  • Adult
  • Aged
  • Androgens / analysis*
  • Androgens / blood*
  • Androgens / therapeutic use
  • Chromatography / methods*
  • Cross-Sectional Studies
  • Diatomaceous Earth
  • Female
  • Humans
  • Middle Aged
  • Postmenopause
  • Premenopause
  • Radioimmunoassay / methods*
  • Solvents
  • Testosterone / analysis*
  • Testosterone / blood*
  • Testosterone / therapeutic use

Substances

  • Androgens
  • Solvents
  • Testosterone
  • Diatomaceous Earth