DNA nicking by HinP1I endonuclease: bending, base flipping and minor groove expansion

Nucleic Acids Res. 2006 Feb 9;34(3):939-48. doi: 10.1093/nar/gkj484. Print 2006.

Abstract

HinP1I recognizes and cleaves the palindromic tetranucleotide sequence G downward arrowCGC in DNA. We report three structures of HinP1I-DNA complexes: in the presence of Ca(2+) (pre-reactive complex), in the absence of metal ion (binary complex) and in the presence of Mg(2+) (post-reactive complex). HinP1I forms a back-to-back dimer with two active sites and two DNA duplexes bound on the outer surfaces of the dimer facing away from each other. The 10 bp DNA duplexes undergo protein-induced distortions exhibiting features of A-, B- and Z-conformations: bending on one side (by intercalation of a phenylalanine side chain into the major groove), base flipping on the other side of the recognition site (by expanding the step rise distance of the local base pair to Z-form) and a local A-form conformation between the two central C:G base pairs of the recognition site (by binding of the N-terminal helix in the minor groove). In the pre- and post-reactive complexes, two metals (Ca(2+) or Mg(2+)) are found in the active site. The enzyme appears to cleave DNA sequentially, hydrolyzing first one DNA strand, as seen in the post-reactive complex in the crystalline state, and then the other, as supported by the observation that, in solution, a nicked DNA intermediate accumulates before linearization.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Binding Sites
  • Calcium / chemistry
  • Catalysis
  • DNA / chemistry*
  • DNA / metabolism
  • Deoxyribonucleases, Type II Site-Specific / chemistry*
  • Deoxyribonucleases, Type II Site-Specific / metabolism
  • Dimerization
  • Models, Molecular
  • Nucleic Acid Conformation
  • Protein Binding

Substances

  • DNA
  • Deoxyribonucleases, Type II Site-Specific
  • GCGC-specific type II deoxyribonucleases
  • Calcium

Associated data

  • PDB/2FKC
  • PDB/2FKH
  • PDB/2FL3
  • PDB/2FLC