Regioselectivity in the Sonogashira coupling of 4,6-dichloro-2-pyrone

Org Biomol Chem. 2006 Apr 7;4(7):1213-6. doi: 10.1039/b518232h. Epub 2006 Feb 21.

Abstract

The Sonogashira cross-coupling of 4,6-dichloro-2-pyrone with terminal acetylenes proceeds in good yields and high regioselectivity for the 6-position; dibenzylidene acetone (dba) type ligands play a non-innocent role in reactions mediated by Pd(dba)2/PPh3; theoretical studies indicate that C-6 oxidative addition is favoured both kinetically and thermodynamically.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkynes / chemistry*
  • Kinetics
  • Magnetic Resonance Spectroscopy
  • Models, Molecular
  • Molecular Conformation
  • Pyrones / chemistry*

Substances

  • Alkynes
  • Pyrones