Crystallization and preliminary X-ray diffraction analysis of rat protein tyrosine phosphatase eta

Acta Crystallogr Sect F Struct Biol Cryst Commun. 2006 Sep 1;62(Pt 9):923-5. doi: 10.1107/S1744309106031058. Epub 2006 Aug 26.

Abstract

The rat protein tyrosine phosphatase eta (rPTPeta) is a cysteine-dependent phosphatase which hydrolyzes phosphoester bonds in proteins and other molecules. rPTPeta and its human homologue DEP-1 are involved in neoplastic transformations. Thus, expression of the protein is reduced in all oncogene-transformed thyroid cell lines and is absent in highly malignant thyroid cells. Moreover, consistent with the suggested tumour suppression role of PTPeta, inhibition of the tumorigenic process occurs after its exogenous reconstitution, suggesting that PTPeta might be important for gene therapy of cancers. In this study, the catalytic domain of rPTPeta was produced in Escherichia coli in soluble form and purified to homogeneity. Crystals were obtained by the hanging-drop vapour-diffusion method. Diffraction data were collected to 1.87 A resolution. The crystal belongs to space group P2(1)2(1)2(1), with unit-cell parameters a = 46.46, b = 63.07, c = 111.64 A, and contains one molecule per asymmetric unit.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Catalytic Domain
  • Crystallization
  • Crystallography, X-Ray
  • Escherichia coli / genetics
  • Protein Subunits / chemistry*
  • Protein Subunits / isolation & purification
  • Protein Tyrosine Phosphatases / chemistry*
  • Protein Tyrosine Phosphatases / isolation & purification
  • Rats
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / isolation & purification

Substances

  • Protein Subunits
  • Recombinant Proteins
  • Protein Tyrosine Phosphatases
  • phosphotyrosine phosphatase eta

Associated data

  • PDB/2AHS