A non-isotopic in vitro assay for histone acetylation

J Biotechnol. 2007 Sep 15;131(3):253-60. doi: 10.1016/j.jbiotec.2007.07.498. Epub 2007 Jul 12.

Abstract

We describe a simple, robust, and relatively inexpensive non-radioactive in vitro assay for measuring histone acetyl-transferase activity. The assay takes advantage of easy to purify recombinant E. coli-derived fusion proteins containing the NH(2)-terminal tails of histones H3 and H4 linked to epitope-tagged maltose-binding protein (MBP), and immunoblotting with antibodies specific to acetylated H3 and H4. Here we show the specificity and dynamic range of this assay for the histone acetyl-transferases, p300 and PCAF. This assay may be adapted readily for other substrates by simply generating new fusion proteins and for other acetyl-transferases by modifying reaction conditions.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Acetylation
  • Animals
  • Biological Assay / methods*
  • Epitope Mapping
  • Histones / chemistry*
  • Immunoblotting / methods*
  • Isotope Labeling
  • Mice
  • Mice, Inbred C3H
  • p300-CBP Transcription Factors / analysis*

Substances

  • Histones
  • p300-CBP Transcription Factors
  • p300-CBP-associated factor