Cellular uptake and cytotoxicity of shell crosslinked stearic acid-grafted chitosan oligosaccharide micelles encapsulating doxorubicin

Eur J Pharm Biopharm. 2008 May;69(1):117-25. doi: 10.1016/j.ejpb.2007.09.018. Epub 2007 Oct 5.

Abstract

Stearic acid-grafted chitosan oligosaccharide (CSO-SA) with 3.48% amino-substituted degree (SD%) was synthesized by coupling reaction. The CSO-SA could self-aggregate to form micelle with a critical micelle concentration (CMC) at 0.035 mg/mL in the aqueous phase. The CSO-SA self-aggregate micelles indicated spatial structure with multi-hydrophobic core. One CSO-SA chain could form 2.8 hydrophobic cores. Cellular uptakes of CSO-SA micelles by using A549, LLC, and SKOV3 cells as model tumor cell lines showed the faster cellular internalization of CSO-SA micelles, and the cellular uptakes on the LLC and SKOV3 cells were higher than that on the A549 cells. Doxorubicin (DOX) was then used as a model drug to incorporate into CSO-SA micelles. To reduce the initial burst drug release from CSO-SA micelles loading DOX (CSO-SA/DOX), the shell of CSO-SA micelles was crosslinked by glutaraldehyde. The shell crosslinking of CSO-SA micelles reduced the micelle size and surface potential, but it did not significantly affect the cellular uptake and drug encapsulation efficiency of CSO-SA micelles. The cellular inhibition experiments demonstrated that the cytotoxicity of DOX was increased by the encapsulation of CSO-SA micelles. CSO-SA/DOX displayed the best antitumor efficacy in SKOV3 cell line due to the higher cellular uptake percentage of CSO-SA micelles and the lower sensitivity of free drug to the cells. The cytotoxicities of shell crosslinked CSO-SA/DOX were highly enhanced in all cell lines than those of unmodified CSO-SA/DOX.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biocompatible Materials / chemistry
  • Cell Line, Tumor
  • Chemistry, Pharmaceutical / methods
  • Chitosan / chemistry*
  • Cross-Linking Reagents / pharmacology
  • Doxorubicin / administration & dosage*
  • Doxorubicin / chemistry
  • Drug Carriers / chemistry*
  • Drug Delivery Systems*
  • Humans
  • Micelles*
  • Oligosaccharides / chemistry
  • Solvents / chemistry
  • Stearic Acids / chemistry*
  • Technology, Pharmaceutical / methods
  • Time Factors

Substances

  • Biocompatible Materials
  • Cross-Linking Reagents
  • Drug Carriers
  • Micelles
  • Oligosaccharides
  • Solvents
  • Stearic Acids
  • stearic acid
  • Doxorubicin
  • Chitosan