Zinc binding ligands and cellular zinc trafficking: apo-metallothionein, glutathione, TPEN, proteomic zinc, and Zn-Sp1

J Inorg Biochem. 2008 Mar;102(3):489-99. doi: 10.1016/j.jinorgbio.2007.10.030. Epub 2007 Nov 28.

Abstract

Many cell types contain metal-ion unsaturated metallothionein (MT). Considering the Zn(2+) binding affinity of metallothionein, the existence of this species in the intracellular environment constitutes a substantial "thermodynamic sink". Indeed, the mM concentration of glutathione may be thought of in the same way. In order to understand how apo-MT and the rest of the Zn-proteome manage to co-exist, experiments examined the in vitro reactivity of Zn-proteome with apo-MT, glutathione (GSH), and a series of common Zn(2+) chelating agents including N,N,N',N'-(2-pyridylethyl)ethylenediammine (TPEN), EDTA, and [(2,2'-oxyproplylene-dinitrilo]tetraacetic acid (EGTA). Less than 10% of Zn-proteome from U87mg cells reacted with apo-MT or GSH. In contrast, each of the synthetic chelators was 2-3 times more reactive. TPEN, a cell permeant reagent, also reacted rapidly with both Zn-proteome and Zn-MT in LLC-PK(1) cells. Taking a specific zinc finger protein for further study, apo-MT, GSH, and TPEN inhibited the binding of Zn(3)-Sp1 with its cognate DNA site (GC-1) in the sodium-glucose co-transporter promoter of mouse kidney. In contrast, preformation of Zn(3)-Sp1-(GC-1) prevented reaction with apo-MT and GSH; TPEN remained active but at a higher concentration. Whereas, Zn(3)-Sp1 is active in cells containing apo-MT and GSH, exposure of LLC-PK(1) cells to TPEN for 24h largely inactivated its DNA binding activity. The results help to rationalize the steady state presence of cellular apo-MT in the midst of the many, diverse members of the Zn-proteome. They also show that TPEN is a robust intracellular chelator of proteomic Zn(2+).

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Biological Transport
  • Carrier Proteins / metabolism*
  • Cell Line
  • Cell Line, Tumor
  • Cells, Cultured
  • Chromatography, Gel
  • Electrophoretic Mobility Shift Assay
  • Ethylenediamines / metabolism*
  • Glutathione / metabolism*
  • Humans
  • Metallothionein / metabolism*
  • Protein Binding
  • Rabbits
  • Sp1 Transcription Factor / metabolism*
  • Zinc / metabolism*

Substances

  • Carrier Proteins
  • Ethylenediamines
  • Sp1 Transcription Factor
  • zinc thionein
  • zinc-binding protein
  • Metallothionein
  • Glutathione
  • Zinc
  • N,N,N',N'-tetrakis(2-pyridylmethyl)ethylenediamine