Role of N-terminal amino acids in the potency of anthrax lethal factor

PLoS One. 2008 Sep 3;3(9):e3130. doi: 10.1371/journal.pone.0003130.

Abstract

Anthrax lethal factor (LF) is a Zn(+2)-dependent metalloprotease that cleaves several MAPK kinases and is responsible for the lethality of anthrax lethal toxin (LT). We observed that a recombinant LF (LF-HMA) which differs from wild type LF (LF-A) by the addition of two residues (His-Met) to the native Ala (A) terminus as a result of cloning manipulations has 3-fold lower potency toward cultured cells and experimental animals. We hypothesized that the "N-end rule", which relates the half-life of proteins in cells to the identity of their N-terminal residue, might be operative in the case of LF, so that the N-terminal residue of LF would determine the cytosolic stability and thereby the potency of LF. Mutational studies that replaced the native N-terminal residue of LF with known N-end rule stabilizing or destabilizing residues confirmed that the N-terminal residue plays a significant role in determining the potency of LT for cultured cells and experimental animals. The fact that a commercially-available LF preparation (LF-HMA) that is widely used in basic research studies and for evaluation of vaccines and therapeutics is 3-fold less potent than native LF (LF-A) should be considered when comparing published studies and in the design of future experiments.

Publication types

  • Research Support, N.I.H., Intramural

MeSH terms

  • Amino Acids / chemistry*
  • Animals
  • Anthrax
  • Antigens, Bacterial / chemistry*
  • Antigens, Bacterial / metabolism*
  • Bacterial Toxins / chemistry*
  • Bacterial Toxins / metabolism*
  • CHO Cells
  • Cricetinae
  • Cricetulus
  • Factor Xa / chemistry
  • Female
  • MAP Kinase Signaling System
  • Mice
  • Protein Binding
  • Protein Structure, Tertiary
  • Rats
  • Rats, Inbred F344
  • Zinc / chemistry

Substances

  • Amino Acids
  • Antigens, Bacterial
  • Bacterial Toxins
  • anthrax toxin
  • Factor Xa
  • Zinc