Radio-copper-labeled Cu-ATSM: an indicator of quiescent but clonogenic cells under mild hypoxia in a Lewis lung carcinoma model

Nucl Med Biol. 2009 May;36(4):419-26. doi: 10.1016/j.nucmedbio.2009.01.016. Epub 2009 Mar 26.

Abstract

The purpose of this study is to reveal characteristics of (64)Cu-labeled diacetyl-bis(N(4)-methylthiosemicarbazone) ([(64)Cu]Cu-ATSM) during cell proliferation and hypoxia by autoradiography imaging and immunohistochemical staining.

Methods: The intratumoral distributions of [(64)Cu]Cu-ATSM and [(18)F]-2-fluoro-2-deoxy-D-glucose ([(18)F]FDG) in mice implanted with Lewis lung carcinoma (LLC1) tumor cells according to dual autoradiography were compared with the immunohistochemical staining patterns of proliferating markers [Ki-67 and 5-bromo-2'-deoxyuridine (BrdU)] and a hypoxic marker (pimonidazole). A clonogenic assay was performed using the cells of LLC1 tumor-implanted mice, and it was compared with the distribution of [(64)Cu]Cu-ATSM.

Results: [(64)Cu]Cu-ATSM mainly accumulated at the edge of tumors, whereas [(18)F]FDG was distributed inside the tumor and inside the [(64)Cu]Cu-ATSM accumulation. The number of Ki-67-positive cells/area tended to increase with [(18)F]FDG accumulation and decrease with [(64)Cu]Cu-ATSM accumulation. On the other hand, the number of BrdU-positive cells/area was negatively correlated with [(18)F]FDG accumulation and positively correlated with [(64)Cu]Cu-ATSM accumulation. High [(64)Cu]Cu-ATSM accumulation was found outside the high-[(18)F]FDG-accumulation and pimonidazole-positive regions. Colony formation ability was significantly higher in the tumor cells obtained from high-[(64)Cu]Cu-ATSM-accumulation regions than the cells from the intermediate- and the low-accumulation regions.

Conclusion: [(64)Cu]Cu-ATSM accumulation regions in tumor cells indicate quiescent but clonogenic tumor cells under mild hypoxia. [(64)Cu]Cu-ATSM could play an important role in planning appropriate tumor radiotherapy.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Autoradiography
  • Bromodeoxyuridine / immunology
  • Carcinoma, Lewis Lung / complications*
  • Carcinoma, Lewis Lung / metabolism
  • Carcinoma, Lewis Lung / pathology*
  • Cell Proliferation
  • Colony-Forming Units Assay
  • Coordination Complexes
  • Copper Radioisotopes / chemistry*
  • Disease Models, Animal
  • Fluorodeoxyglucose F18 / metabolism
  • Hypoxia / complications*
  • Hypoxia / metabolism
  • Hypoxia / pathology*
  • Image Processing, Computer-Assisted
  • Immunohistochemistry
  • Ki-67 Antigen / immunology
  • Male
  • Mice
  • Nitroimidazoles / chemistry
  • Nitroimidazoles / immunology
  • Organometallic Compounds / chemistry
  • Organometallic Compounds / metabolism*
  • Positron-Emission Tomography
  • Staining and Labeling
  • Thiosemicarbazones / chemistry
  • Thiosemicarbazones / metabolism*

Substances

  • Coordination Complexes
  • Copper Radioisotopes
  • Ki-67 Antigen
  • Nitroimidazoles
  • Organometallic Compounds
  • Thiosemicarbazones
  • copper (II) diacetyl-di(N(4)-methylthiosemicarbazone)
  • Fluorodeoxyglucose F18
  • pimonidazole
  • Bromodeoxyuridine