Structure of bovine pancreatic ribonuclease complexed with uridine 5'-monophosphate at 1.60 A resolution

Acta Crystallogr Sect F Struct Biol Cryst Commun. 2010 Feb 1;66(Pt 2):113-20. doi: 10.1107/S174430910905194X. Epub 2010 Jan 26.

Abstract

Bovine pancreatic ribonuclease A (RNase A) was crystallized from a mixture of small molecules containing basic fuchsin, tobramycin and uridine 5'-monophosphate (U5P). Solution of the crystal structure revealed that the enzyme was selectively bound to U5P, with the pyrimidine ring of U5P residing in the pyrimidine-binding site at Thr45. The structure was refined to an R factor of 0.197 and an R(free) of 0.253.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Animals
  • Binding Sites
  • Cattle
  • Crystallography, X-Ray
  • Ligands
  • Models, Molecular
  • Mutation
  • Protein Binding
  • Protein Structure, Tertiary
  • Ribonuclease, Pancreatic / chemistry*
  • Ribonuclease, Pancreatic / genetics
  • Ribonuclease, Pancreatic / metabolism
  • Uridine Monophosphate / chemistry*
  • Uridine Monophosphate / metabolism

Substances

  • Ligands
  • Uridine Monophosphate
  • Ribonuclease, Pancreatic