Effects of metal and the phytyl chain on chlorophyll derivatives: physicochemical evaluation for photodynamic inactivation of microorganisms

Photochem Photobiol. 2011 Jul-Aug;87(4):884-94. doi: 10.1111/j.1751-1097.2011.00935.x. Epub 2011 May 27.

Abstract

Chlorophyll compounds and their derivatives containing metal or phytyl chain can be used as photosensitizer in photodynamic inactivation of microorganisms (PDI). So, the physicochemical properties and antimicrobial effect of chlorophyll derivatives were investigated: Mg-chlorophyll (Mg-Chl), Zn-chlorophyll (Zn-Chl), Zn-chlorophyllide (Zn-Chlde), Cu-chlorophyll (Cu-Chl), pheophytin (Pheo) and pheophorbide (Pheid). The photobleaching experiments showed photostability according to Cu-Chl > Pheo ∼ Pheid ≫ Zn-Chl ∼ Zn-Chlde > Mg-Chl. This order was discussed in terms of metal and the phytyl chain presences. Pheid and Zn-Chl in aqueous Tween 80 solution exhibited highest singlet oxygen yield compared with the other derivatives. Chlorophyll derivatives (CD) with phytyl chain was limited by the self-aggregation phenomenon at high concentrations, even in micellar systems (Tween 80 and P-123). The antimicrobial effect of CD derivatives was investigated against Staphylococcus aureus, Escherichia coli, Candida albicans and Artemia salina. Pheid showed the best results against all organisms tested, Zn-Chlde was an excellent bactericide in the dark and Cu-Chl had no PDI effect. No correlation with CD uptake by microorganisms and darkness cytotoxicity was found. The physicochemical properties allied to bioassays results indicate that Mg-Chl, Pheo, Zn-Chl and Pheid are good candidates for PDI.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Anti-Infective Agents / chemistry
  • Anti-Infective Agents / pharmacology*
  • Artemia / drug effects
  • Artemia / growth & development
  • Artemia / radiation effects
  • Candida albicans / drug effects
  • Candida albicans / growth & development
  • Candida albicans / radiation effects
  • Chlorophyll / analogs & derivatives
  • Chlorophyll / chemistry
  • Chlorophyll / pharmacology*
  • Copper / chemistry
  • Copper / metabolism
  • Escherichia coli / drug effects
  • Escherichia coli / growth & development
  • Escherichia coli / radiation effects
  • Kinetics
  • Magnesium / chemistry
  • Magnesium / metabolism
  • Micelles
  • Pheophytins / chemistry
  • Pheophytins / pharmacology*
  • Photobleaching / radiation effects*
  • Photochemotherapy / methods*
  • Photosensitizing Agents / chemistry
  • Photosensitizing Agents / pharmacology*
  • Polysorbates / chemistry
  • Singlet Oxygen
  • Spectrometry, Fluorescence
  • Staphylococcus aureus / drug effects
  • Staphylococcus aureus / growth & development
  • Staphylococcus aureus / radiation effects
  • Water
  • Zinc / chemistry
  • Zinc / metabolism

Substances

  • Anti-Infective Agents
  • Micelles
  • Pheophytins
  • Photosensitizing Agents
  • Polysorbates
  • Water
  • Chlorophyll
  • Singlet Oxygen
  • Copper
  • Magnesium
  • Zinc