N@C60-porphyrin: a dyad of two radical centers

J Am Chem Soc. 2012 Feb 1;134(4):1938-41. doi: 10.1021/ja209763u. Epub 2012 Jan 24.

Abstract

Dyads of endohedral nitrogen fullerene and porphyrin have been synthesized. In the two-radical-center dyad, the copper(II) tetraphenylporphyrin suppressed the electron spin resonance (ESR) signal of N@C(60) through intramolecular dipolar coupling with a strength of 27.0 MHz. Demetalation of the metalloporphyrin moiety of the dyad, which effectively turned the two-radical-center dyad into a single-radical-center dyad, recovered 82% of the ESR signal of N@C(60). Such mechanism of switching a spin state on and off could find use in molecular spintronics applications.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Copper / chemistry*
  • Free Radicals / chemical synthesis
  • Free Radicals / chemistry
  • Fullerenes / chemistry*
  • Metalloporphyrins / chemical synthesis
  • Metalloporphyrins / chemistry*
  • Molecular Structure
  • Nitrogen / chemistry*
  • Porphyrins / chemistry*

Substances

  • Free Radicals
  • Fullerenes
  • Metalloporphyrins
  • Porphyrins
  • Copper
  • Nitrogen
  • fullerene C60