Structural study on the architecture of the bacterial ATP synthase Fo motor

Proc Natl Acad Sci U S A. 2012 Jul 24;109(30):E2050-6. doi: 10.1073/pnas.1203971109. Epub 2012 Jun 26.

Abstract

We purified the F(o) complex from the Ilyobacter tartaricus Na(+)-translocating F(1)F(o)-ATP synthase and performed a biochemical and structural study. Laser-induced liquid bead ion desorption MS analysis demonstrates that all three subunits of the isolated F(o) complex were present and in native stoichiometry (ab(2)c(11)). Cryoelectron microscopy of 2D crystals yielded a projection map at a resolution of 7.0 Å showing electron densities from the c(11) rotor ring and up to seven adjacent helices. A bundle of four helices belongs to the stator a-subunit and is in contact with c(11). A fifth helix adjacent to the four-helix bundle interacts very closely with a c-subunit helix, which slightly shifts its position toward the ring center. Atomic force microscopy confirms the presence of the F(o) stator, and a height profile reveals that it protrudes less from the membrane than c(11). The data limit the dimensions of the subunit a/c-ring interface: Three helices from the stator region are in contact with three c(11) helices. The location and distances of the stator helices impose spatial restrictions on the bacterial F(o) complex.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cryoelectron Microscopy
  • Crystallization
  • Fusobacteria / enzymology*
  • Immunohistochemistry
  • Mass Spectrometry
  • Microscopy, Atomic Force
  • Models, Molecular*
  • Protein Conformation*
  • Protein Subunits / chemistry
  • Proton-Translocating ATPases / chemistry*
  • Proton-Translocating ATPases / isolation & purification

Substances

  • Protein Subunits
  • Proton-Translocating ATPases