Molecular recognition of complex-type biantennary N-glycans by protein receptors: a three-dimensional view on epitope selection by NMR

J Am Chem Soc. 2013 Feb 20;135(7):2667-75. doi: 10.1021/ja3104928. Epub 2013 Feb 5.

Abstract

The current surge in defining glycobiomarkers by applying lectins rekindles interest in definition of the sugar-binding sites of lectins at high resolution. Natural complex-type N-glycans can present more than one potential binding motif, posing the question of the actual mode of interaction when interpreting, for example, lectin array data. By strategically combining N-glycan preparation with saturation-transfer difference NMR and modeling, we illustrate that epitope recognition depends on the structural context of both the sugar and the lectin (here, wheat germ agglutinin and a single hevein domain) and cannot always be predicted from simplified model systems studied in the solid state. We also monitor branch-end substitutions by this strategy and describe a three-dimensional structure that accounts for the accommodation of the α2,6-sialylated terminus of a biantennary N-glycan by viscumin. In addition, we provide a structural explanation for the role of terminal α2,6-sialylation in precluding the interaction of natural N-glycans with lectin from Maackia amurensis . The approach described is thus capable of pinpointing lectin-binding motifs in natural N-glycans and providing detailed structural explanations for lectin selectivity.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antimicrobial Cationic Peptides / chemistry
  • Binding Sites
  • Epitopes / chemistry*
  • Epitopes / metabolism
  • Ligands
  • Magnetic Resonance Spectroscopy
  • Models, Molecular
  • Plant Lectins / chemistry
  • Polysaccharides / chemistry*
  • Polysaccharides / metabolism

Substances

  • Antimicrobial Cationic Peptides
  • Epitopes
  • Ligands
  • Plant Lectins
  • Polysaccharides
  • hevein