Novel porous Al2O3-SiO2-TiO2 bone grafting materials: formation and characterization

J Biomater Appl. 2014 Feb;28(6):813-24. doi: 10.1177/0885328213483634. Epub 2013 Apr 16.

Abstract

The present article deals with the development of 3D porous scaffolds for bone grafting. They were prepared based on rapid fluid infiltration of Al2O3-SiO2 sol into a polyethylene non-woven fabric template structure. Titanium dioxide in concentration equal to 5 wt% was added to the Al2O3-SiO2 mixture to produce Al2O3-SiO2-TiO2 composite scaffolds. The prepared scaffolds are characterized by means of X-ray diffraction, scanning electron microscopy and three-point bending test techniques. The bioactivity of the produced bodies is discussed, including the in vitro and in vivo assessments. The produced scaffolds exhibit mean total porosity of 66.0% and three-point bending strength of 7.1 MPa. In vitro studies showed that MG-63 osteoblast-like cells attach and spread on the scaffolds surfaces. Furthermore, cells grew through the scaffolds and start to produce extra-cellular matrix. Additionally, in vivo studies revealed the ability of the porous scaffolds to regenerate bone tissue in femur defects of albino rats 5 months post surgery. Histological analysis showed that the defect is almost entirely filled with new bone. The formed bone is characterized as a mature bone. The produced bone grafts are intended to be used as bone substitute or bone filler as their degradation products caused no inflammatory effects.

Keywords: Bone grafting; bioceramics; in vitro; in vivo; porous materials.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aluminum Oxide / chemistry*
  • Animals
  • Biocompatible Materials / chemistry
  • Bone Transplantation*
  • Cell Line
  • Male
  • Microscopy, Electron, Scanning
  • Rats
  • Rats, Sprague-Dawley
  • Silicon Dioxide / chemistry*
  • Tissue Scaffolds
  • Titanium / chemistry*
  • X-Ray Diffraction

Substances

  • Biocompatible Materials
  • titanium dioxide
  • Silicon Dioxide
  • Titanium
  • Aluminum Oxide