Processive ATP-driven substrate disassembly by the N-ethylmaleimide-sensitive factor (NSF) molecular machine

J Biol Chem. 2013 Aug 9;288(32):23436-45. doi: 10.1074/jbc.M113.476705. Epub 2013 Jun 17.

Abstract

SNARE proteins promote membrane fusion by forming a four-stranded parallel helical bundle that brings the membranes into close proximity. Post-fusion, the complex is disassembled by an AAA+ ATPase called N-ethylmaleimide-sensitive factor (NSF). We present evidence that NSF uses a processive unwinding mechanism to disassemble SNARE proteins. Using a real-time disassembly assay based on fluorescence dequenching, we correlate NSF-driven disassembly rates with the SNARE-activated ATPase activity of NSF. Neuronal SNAREs activate the ATPase rate of NSF by ∼26-fold. One SNARE complex takes an average of ∼5 s to disassemble in a process that consumes ∼50 ATP. Investigations of substrate requirements show that NSF is capable of disassembling a truncated SNARE substrate consisting of only the core SNARE domain, but not an unrelated four-stranded coiled-coil. NSF can also disassemble an engineered double-length SNARE complex, suggesting a processive unwinding mechanism. We further investigated processivity using single-turnover experiments, which show that SNAREs can be unwound in a single encounter with NSF. We propose a processive helicase-like mechanism for NSF in which ∼1 residue is unwound for every hydrolyzed ATP molecule.

Keywords: AAA+ ATPase; ATPases; Exocytosis; Fluorescence; Mechanochemical Coupling; Membrane Fusion; Molecular Motors; Remodeling; Translocase; Unfoldase.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adenosine Triphosphate / chemistry*
  • Adenosine Triphosphate / genetics
  • Adenosine Triphosphate / metabolism
  • Humans
  • N-Ethylmaleimide-Sensitive Proteins / chemistry*
  • N-Ethylmaleimide-Sensitive Proteins / genetics
  • N-Ethylmaleimide-Sensitive Proteins / metabolism
  • Protein Structure, Tertiary
  • SNARE Proteins / chemistry*
  • SNARE Proteins / genetics
  • SNARE Proteins / metabolism

Substances

  • SNARE Proteins
  • Adenosine Triphosphate
  • N-Ethylmaleimide-Sensitive Proteins