Polyglycerol-coated nanodiamond as a macrophage-evading platform for selective drug delivery in cancer cells

Biomaterials. 2014 Jul;35(20):5393-5406. doi: 10.1016/j.biomaterials.2014.03.041. Epub 2014 Apr 8.

Abstract

A successful targeted drug delivery device for cancer chemotherapy should ideally be able to avoid non-specific uptake by nonmalignant cells, particularly the scavenging monocyte-macrophage system as well as targeting efficacy to bring the drug preferentially into tumor cells. To this purpose, we developed a platform based on detonation nanodiamond (dND) with hyperbranched polyglycerol (PG) coating (dND-PG). dND-PG was first demonstrated to evade non-specific cell uptake, particularly by macrophages (U937). RGD targeting peptide was then conjugated to dND-PG through multistep organic transformations to yield dND-PG-RGD that still evaded macrophage uptake but was preferentially taken up by targeted A549 cancer cells (expressing RGD peptide receptors). dND-PG and dND-PG-RGD showed good aqueous solubility and cytocompatibitlity. Subsequently, the anticancer agent doxorubicin (DOX) was loaded through acid-labile hydrazone linkage to yield dND-PG-DOX and dND-PG-RGD-DOX. Their cellular uptake and cytotoxicity were compared against DOX in A549 cells and U937 macrophages. It was found that dND-PG-DOX uptake was substantially reduced, displaying little toxicity in either type of cells by virtue of PG coating, whereas dND-PG-RGD-DOX exerted selective toxicity to A549 cells over U937 macrophages that are otherwise highly sensitive to DOX. Finally, dND-PG was demonstrated to have little influence on U937 macrophage cell functions, except for a slight increase of TNF-α production in resting U937 macrophages. dND-PG is a promising drug carrier for realization of highly selective drug delivery in tumor cells through specific uptake mechanisms, with minimum uptake in and influence on macrophages.

Keywords: Cancer cells; Coating; Detonation nanodiamond; Polyglycerol; RGD peptide; Selective delivery.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antibiotics, Antineoplastic / pharmacology
  • Cell Line, Tumor
  • Doxorubicin / pharmacology
  • Drug Carriers / chemistry
  • Drug Delivery Systems / methods*
  • Glycerol / chemistry*
  • Glycerol / pharmacology
  • Humans
  • Liposomes
  • Macrophages / metabolism*
  • Nanodiamonds / chemistry*
  • Neoplasms / therapy
  • Oligopeptides / pharmacology
  • Phagocytosis
  • Polymers / chemistry*
  • Polymers / pharmacology
  • Reactive Oxygen Species / metabolism
  • Tumor Necrosis Factor-alpha / metabolism
  • U937 Cells

Substances

  • Antibiotics, Antineoplastic
  • Drug Carriers
  • Liposomes
  • Nanodiamonds
  • Oligopeptides
  • Polymers
  • Reactive Oxygen Species
  • Tumor Necrosis Factor-alpha
  • polyglycerol
  • arginyl-glycyl-aspartic acid
  • Doxorubicin
  • Glycerol