Identification of Small Inhibitory Molecules Targeting the Bfl-1 Anti-Apoptotic Protein That Alleviates Resistance to ABT-737

J Biomol Screen. 2014 Aug;19(7):1035-46. doi: 10.1177/1087057114534070. Epub 2014 May 8.

Abstract

One approach currently being developed in anticancer drug discovery is to search for small compounds capable of occupying and blocking the hydrophobic pocket of anti-apoptotic Bcl-2 family members necessary for interacting with pro-apoptotic proteins. Such an approach led to the discovery of several compounds, such as ABT-737 (which interacts with Bcl-2, Bcl-xl, and Bcl-w) or the latest one, ABT-199, that selectively targets Bcl-2 protein. The efficacy of those compounds is, however, limited by the expression of two other anti-apoptotic Bcl-2 members, Mcl-1 and Bfl-1. Based on the role of Bfl-1 in cancer, especially in chemoresistance associated with its overexpression in B-cell malignancies, we searched for modulators of protein-protein interaction through a high-throughput screening of a designed chemical library with relaxed drug-like properties to identify small molecules targeting Bfl-1 anti-apoptotic protein. We found two compounds that display electrophilic functions, interact with Bfl-1, inhibit Bfl-1 protective activity, and promote cell death of malignant B cells. Of particular interest, we observed a synergistic effect of those compounds with ABT-737 in Bfl-1 overexpressing lymphoma cell lines. Our results provide the basis for the development of Bfl-1 specific antagonists for antitumor therapies.

Keywords: Bcl-2; Bfl-1; apoptosis; high-throughput screening; protein–protein interaction inhibitors.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antineoplastic Agents / chemistry*
  • Apoptosis Regulatory Proteins
  • Apoptosis*
  • Biphenyl Compounds / pharmacology*
  • Bridged Bicyclo Compounds, Heterocyclic / chemistry
  • Cell Line, Tumor
  • Drug Discovery / methods*
  • Drug Resistance*
  • Glutathione / chemistry
  • Glutathione Transferase / metabolism
  • High-Throughput Screening Assays / methods
  • Humans
  • Lymphoma / drug therapy*
  • Minor Histocompatibility Antigens
  • Molecular Conformation
  • Nitrophenols / pharmacology*
  • Piperazines / pharmacology
  • Protein Binding
  • Protein Interaction Mapping
  • Proto-Oncogene Proteins c-bcl-2 / antagonists & inhibitors*
  • Spectrometry, Fluorescence
  • Sulfonamides / chemistry
  • Sulfonamides / pharmacology*

Substances

  • ABT-737
  • Antineoplastic Agents
  • Apoptosis Regulatory Proteins
  • BCL2-related protein A1
  • Biphenyl Compounds
  • Bridged Bicyclo Compounds, Heterocyclic
  • Minor Histocompatibility Antigens
  • Nitrophenols
  • Piperazines
  • Proto-Oncogene Proteins c-bcl-2
  • Sulfonamides
  • Glutathione Transferase
  • Glutathione
  • venetoclax