Development of a universal anti-adalimumab antibody standard for interlaboratory harmonization

Ther Drug Monit. 2014 Oct;36(5):669-73. doi: 10.1097/FTD.0000000000000074.

Abstract

Background: Therapeutic drug monitoring of adalimumab (ADM) has been introduced recently. When no detectable ADM serum concentrations can be found, the formation of antidrug antibodies (ADA) should be investigated. A variety of assays to measure the occurrence of ADA have been developed. Results are expressed as arbitrary units or as a titration value. The aim was to develop a monoclonal antibody (MA) that could serve as a universal calibrator to quantify the amount of ADA in ADM-treated patients.

Methods: Hybridoma technology was used to generate a MA toward ADM. The functionality of the MA was tested in a bridging enzyme linked immunosorbent assay (ELISA) setup and in a cell-based assay. Sera from 25 anti-tumor necrosis factor naive patients with inflammatory bowel disease were used to determine the cutoff values. Sera from 9 ADM-treated patients with inflammatory bowel disease, with undetectable serum concentrations of ADM were used to quantify the ADA response.

Results: In this study, MA-ADM6A10, an IgG1 that can be used as a calibrator in both an ELISA to quantify the amount of binding antibodies and in a cell-based assay to quantify the amount of neutralizing antibodies, was generated. Combining the results of both assays showed that the sera with high concentrations of anti-ADM binding antibodies also had the highest neutralizing capacity.

Conclusions: The availability of a universal calibrator could facilitate the interlaboratory harmonization of antibody titers in patients who develop anti-adalimumab antibodies.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adalimumab
  • Anti-Inflammatory Agents / blood
  • Anti-Inflammatory Agents / immunology
  • Antibodies / blood*
  • Antibodies / immunology*
  • Antibodies, Monoclonal, Humanized / blood*
  • Antibodies, Monoclonal, Humanized / immunology
  • Cell Line, Tumor
  • Drug Monitoring / methods
  • Fibrosarcoma / metabolism
  • Gene Expression Regulation / physiology
  • Humans
  • Hybridomas / immunology
  • Immunoassay / methods*
  • Immunoglobulin G / immunology*
  • Interleukin-6 / genetics
  • Interleukin-6 / metabolism
  • Laboratories / standards*

Substances

  • Anti-Inflammatory Agents
  • Antibodies
  • Antibodies, Monoclonal, Humanized
  • Immunoglobulin G
  • Interleukin-6
  • Adalimumab