Crystallization and preliminary X-ray diffraction analysis of YidC, a membrane-protein chaperone and insertase from Bacillus halodurans

Acta Crystallogr F Struct Biol Commun. 2014 Aug;70(Pt 8):1056-60. doi: 10.1107/S2053230X14012540. Epub 2014 Jul 23.

Abstract

YidC, a member of the YidC/Oxa1/Alb3 family, inserts proteins into the membrane and facilitates membrane-protein folding in bacteria. YidC plays key roles in both Sec-mediated integration and Sec-independent insertion of membrane proteins. Here, Bacillus halodurans YidC2, which has five transmembrane helices conserved among the other family members, was identified as a target protein for structure determination by a fluorescent size-exclusion chromatography analysis. The protein was overexpressed, purified and crystallized in the lipidic cubic phase. The crystals diffracted X-rays to 2.4 Å resolution and belonged to space group P21, with unit-cell parameters a = 43.9, b = 60.6, c = 58.9 Å, β = 100.3°. The experimental phases were determined by the multiwavelength anomalous diffraction method using a mercury-derivatized crystal.

Keywords: Bacillus halodurans; YidC; lipidic cubic phase; membrane-protein insertase.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacillus / chemistry*
  • Bacillus / enzymology
  • Bacterial Proteins / chemistry*
  • Chromatography, Gel
  • Crystallography, X-Ray
  • Enzymes / chemistry*
  • Molecular Chaperones / chemistry*

Substances

  • Bacterial Proteins
  • Enzymes
  • Molecular Chaperones