Nanowell-based immunoassays for measuring single-cell secretion: characterization of transport and surface binding

Anal Chem. 2014 Dec 2;86(23):11562-9. doi: 10.1021/ac4030297. Epub 2014 Nov 17.

Abstract

Arrays of subnanoliter wells (nanowells) provide a useful system to isolate single cells and analyze their secreted proteins. Two general approaches have emerged: one that uses open arrays and local capture of secreted proteins, and a second (called microengraving) that relies on closed arrays to capture secreted proteins on a solid substrate, which is subsequently removed from the array. However, the design and operating parameters for efficient capture from these two approaches to analyze single-cell secretion have not been extensively considered. Using numerical simulations, we analyzed the operational envelope for both open and closed formats, as a function of the spatial distribution of capture ligands, their affinities for the protein, and the rates of single-cell secretion. Based on these analyses, we present a modified approach to capture secreted proteins in-well for highly active secreting cells. This simple method for in-well detection should facilitate rapid identification of cell lines with high specific productivities.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Animals
  • Binding Sites
  • Chickens
  • Hybridomas / cytology
  • Hybridomas / metabolism*
  • Immunoassay*
  • Immunoglobulin G / analysis*
  • Immunoglobulin G / immunology
  • Nanostructures / chemistry*
  • Ovalbumin / immunology
  • Single-Cell Analysis / methods*
  • Surface Properties

Substances

  • Immunoglobulin G
  • Ovalbumin