β-Strand mimics based on tetrahydropyridazinedione (tpd) peptide stitching

Chem Commun (Camb). 2015 Nov 21;51(90):16259-62. doi: 10.1039/c5cc07189e.

Abstract

Short peptides featuring a tetrahydropyridazinedione (tpd) backbone tether exhibit reduced conformational flexibility external to the heterocyclic constraint. Analysis by NMR, molecular modeling and X-ray crystallography suggests both covalent and non-covalent stabilization of extended peptide conformations. An efficient solid-phase protocol was developed for the synthesis of a new class of β-strand mimics based on oligomeric tpd subunits.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Biomimetic Materials / chemical synthesis*
  • Biomimetic Materials / chemistry*
  • Crystallography, X-Ray
  • Models, Molecular
  • Molecular Conformation
  • Peptides / chemistry*
  • Pyridazines / chemistry*

Substances

  • Peptides
  • Pyridazines