The asymmetric total synthesis of (+)-N-acetyl norloline

Chem Commun (Camb). 2016 Jan 11;52(3):561-3. doi: 10.1039/c5cc07480k. Epub 2015 Nov 5.

Abstract

The asymmetric total synthesis of (+)-N-acetyl norloline, the putative biogenic precursor of all known loline alkaloids, has been achieved in 12 steps from commercially available (R)-glyceraldehyde acetonide. The synthesis relies on the Rassu/Casiraghi's vinylogous aldol reaction, an intramolecular oxa-heteroconjugate addition and a reductive amination to establish the four contiguous stereogenic centers and construct the strained oxygen-bridge under mild conditions.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkaloids / chemical synthesis*
  • Alkaloids / chemistry
  • Bridged-Ring Compounds / chemical synthesis
  • Bridged-Ring Compounds / chemistry*
  • Glyceraldehyde / analogs & derivatives*
  • Glyceraldehyde / chemistry
  • Molecular Structure
  • Oxidation-Reduction

Substances

  • Alkaloids
  • Bridged-Ring Compounds
  • N-acetyl norloline
  • glyceraldehyde acetonide
  • Glyceraldehyde