High-content imaging-based BAC-GFP toxicity pathway reporters to assess chemical adversity liabilities

Arch Toxicol. 2017 Mar;91(3):1367-1383. doi: 10.1007/s00204-016-1781-0. Epub 2016 Jun 29.

Abstract

Adaptive cellular stress responses are paramount in the healthy control of cell and tissue homeostasis and generally activated during toxicity in a chemical-specific manner. Here, we established a platform containing a panel of distinct adaptive stress response reporter cell lines based on BAC-transgenomics GFP tagging in HepG2 cells. Our current panel of eleven BAC-GFP HepG2 reporters together contains (1) upstream sensors, (2) downstream transcription factors and (3) their respective target genes, representing the oxidative stress response pathway (Keap1/Nrf2/Srxn1), the unfolded protein response in the endoplasmic reticulum (Xbp1/Atf4/BiP/Chop) and the DNA damage response (53bp1/p53/p21). Using automated confocal imaging and quantitative single-cell image analysis, we established that all reporters allowed the time-resolved, sensitive and mode-of-action-specific activation of the individual BAC-GFP reporter cell lines as defined by a panel of pathway-specific training compounds. Implementing the temporal pathway activity information increased the discrimination of training compounds. For a set of >30 hepatotoxicants, the induction of Srxn1, BiP, Chop and p21 BAC-GFP reporters correlated strongly with the transcriptional responses observed in cryopreserved primary human hepatocytes. Together, our data indicate that a phenotypic adaptive stress response profiling platform will allow a high throughput and time-resolved classification of chemical-induced stress responses, thus assisting in the future mechanism-based safety assessment of chemicals.

Keywords: Adaptive stress signaling; DILI; High-content imaging.

MeSH terms

  • Chemical and Drug Induced Liver Injury / etiology*
  • Chromosomes, Artificial, Bacterial*
  • DNA Damage / drug effects
  • DNA Damage / genetics
  • Genes, Reporter
  • Green Fluorescent Proteins / analysis*
  • Green Fluorescent Proteins / genetics
  • Green Fluorescent Proteins / metabolism
  • Hep G2 Cells / drug effects
  • Hepatocytes / drug effects
  • Humans
  • Molecular Imaging / methods*
  • Oxidative Stress / drug effects
  • Oxidative Stress / genetics
  • Stress, Physiological / drug effects
  • Stress, Physiological / genetics
  • Toxicity Tests / methods*
  • Unfolded Protein Response / drug effects
  • Unfolded Protein Response / genetics

Substances

  • Green Fluorescent Proteins