A Sensitive and Label-Free Pb(II) Fluorescence Sensor Based on a DNAzyme Controlled G-Quadruplex/Thioflavin T Conformation

Sensors (Basel). 2016 Dec 16;16(12):2155. doi: 10.3390/s16122155.

Abstract

Pb(II) can cause serious damaging effects to human health, and thus, the study of Pb2+ detection methods to sensitively and selectively monitor Pb(II) pollution has significant importance. In this work, we have developed a label-free fluorescence sensing strategy based on a Pb(II) DNAzyme cleavage and the ThT/G-quadruplex complex. In the presence of Pb(II), a G-rich tail was cut and released from the substrate strand, which then would form a G-quadruplex structure by combination with ThT dye. The fluorescence signal increase was then measured for sensitive Pb(II) quantification with a limit of detection of 0.06 nM. Our sensor also demonstrated high selectivity against six different metal ions, which is very important for the analysis of complex samples.

Keywords: DNAzyme; heavy metal ions; lead ion; thioflavin T (ThT).

MeSH terms

  • Benzothiazoles
  • Biosensing Techniques / instrumentation*
  • DNA, Catalytic / chemistry*
  • Fluorescence
  • G-Quadruplexes*
  • Lead / analysis*
  • Limit of Detection
  • Molecular Conformation*
  • Staining and Labeling*
  • Temperature
  • Thiazoles / chemistry*

Substances

  • Benzothiazoles
  • DNA, Catalytic
  • Thiazoles
  • thioflavin T
  • Lead