Alloy-assisted deposition of three-dimensional arrays of atomic gold catalyst for crystal growth studies

Nat Commun. 2017 Dec 8;8(1):2014. doi: 10.1038/s41467-017-02025-x.

Abstract

Large-scale assembly of individual atoms over smooth surfaces is difficult to achieve. A configuration of an atom reservoir, in which individual atoms can be readily extracted, may successfully address this challenge. In this work, we demonstrate that a liquid gold-silicon alloy established in classical vapor-liquid-solid growth can deposit ordered and three-dimensional rings of isolated gold atoms over silicon nanowire sidewalls. We perform ab initio molecular dynamics simulation and unveil a surprising single atomic gold-catalyzed chemical etching of silicon. Experimental verification of this catalytic process in silicon nanowires yields dopant-dependent, massive and ordered 3D grooves with spacing down to ~5 nm. Finally, we use these grooves as self-labeled and ex situ markers to resolve several complex silicon growths, including the formation of nodes, kinks, scale-like interfaces, and curved backbones.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Alloys / chemistry*
  • Catalysis
  • Crystallization
  • Gold / chemistry*
  • Microscopy, Electron, Transmission
  • Nanotechnology / methods
  • Nanowires / chemistry*
  • Nanowires / ultrastructure
  • Photoelectron Spectroscopy
  • Silicon / chemistry*

Substances

  • Alloys
  • Gold
  • Silicon