Glucansucrase (mutant) enzymes from Lactobacillus reuteri 180 efficiently transglucosylate Stevia component rebaudioside A, resulting in a superior taste

Sci Rep. 2018 Jan 24;8(1):1516. doi: 10.1038/s41598-018-19622-5.

Abstract

Steviol glycosides from the leaves of the plant Stevia rebaudiana are high-potency natural sweeteners but suffer from a lingering bitterness. The Lactobacillus reuteri 180 wild-type glucansucrase Gtf180-ΔN, and in particular its Q1140E-mutant, efficiently α-glucosylated rebaudioside A (RebA), using sucrose as donor substrate. Structural analysis of the products by MALDI-TOF mass spectrometry, methylation analysis and NMR spectroscopy showed that both enzymes exclusively glucosylate the Glc(β1→C-19 residue of RebA, with the initial formation of an (α1→6) linkage. Docking of RebA in the active site of the enzyme revealed that only the steviol C-19 β-D-glucosyl moiety is available for glucosylation. Response surface methodology was applied to optimize the Gtf180-ΔN-Q1140E-catalyzed α-glucosylation of RebA, resulting in a highly productive process with a RebA conversion of 95% and a production of 115 g/L α-glucosylated products within 3 h. Development of a fed-batch reaction allowed further suppression of α-glucan synthesis which improved the product yield to 270 g/L. Sensory analysis by a trained panel revealed that glucosylated RebA products show a significant reduction in bitterness, resulting in a superior taste profile compared to RebA. The Gtf180-ΔN-Q1140E glucansucrase mutant enzyme thus is an efficient biocatalyst for generating α-glucosylated RebA variants with improved edulcorant/organoleptic properties.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Diterpenes, Kaurane / chemistry
  • Diterpenes, Kaurane / metabolism*
  • Glycosylation*
  • Glycosyltransferases / genetics*
  • Glycosyltransferases / metabolism*
  • Limosilactobacillus reuteri / enzymology*
  • Magnetic Resonance Spectroscopy
  • Mutant Proteins / genetics
  • Mutant Proteins / metabolism
  • Mutation, Missense
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization
  • Sucrose / metabolism
  • Sweetening Agents / chemistry
  • Sweetening Agents / metabolism*
  • Taste

Substances

  • Diterpenes, Kaurane
  • Mutant Proteins
  • Sweetening Agents
  • Sucrose
  • rebaudioside A
  • Glycosyltransferases
  • alternansucrase