Biochemical study of sortase E2 from Streptomyces mobaraensis and determination of transglutaminase cross-linking sites

FEBS Lett. 2019 Aug;593(15):1944-1956. doi: 10.1002/1873-3468.13466. Epub 2019 Jun 24.

Abstract

Distinct streptomycetes such as Streptomyces mobaraensis produce the protein cross-linking enzyme transglutaminase. Bioinformatic analysis predicted the occurrence of seven sortases exerting transpeptidation reactions similarly to transglutaminase. Here, we report the production and characterization of sortase E2 (Sm-SrtE2) solubilized by removal of its membrane anchor domain. Sm-SrtE2 activity was measured using pentapeptides predicted to be cell wall sorting signals of putative sortase substrate proteins. Preferred linkage to Gly3 by Sm-SrtE2 was in the order LAETG>>LAHTG>>LAQTG~LANTG>LARTG. Chaplin 1 from S. mobaraensis was further demonstrated to be an excellent substrate of both the intrinsic Sm-SrtE2 and transglutaminase. The unexpected discovery showing Gln-62 and Gln-65 of Δ1-50 -Sm-SrtE2 as transglutaminase cross-linking sites suggests that low enzyme stability might be due to anchor domain truncation and a disordered N terminus.

Keywords: Streptomyces mobaraensis; chaplin; glutamine donor proteins; kinetics; sortase; transglutaminase.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aminoacyltransferases / chemistry*
  • Aminoacyltransferases / genetics
  • Aminoacyltransferases / metabolism*
  • Bacterial Proteins / chemistry*
  • Bacterial Proteins / genetics
  • Bacterial Proteins / metabolism*
  • Cell Wall / metabolism
  • Cysteine Endopeptidases / chemistry*
  • Cysteine Endopeptidases / genetics
  • Cysteine Endopeptidases / metabolism*
  • Glutamine / metabolism
  • Oligopeptides / chemistry
  • Oligopeptides / metabolism*
  • Protein Sorting Signals
  • Solubility
  • Streptomyces / enzymology*
  • Transglutaminases / genetics
  • Transglutaminases / metabolism

Substances

  • Bacterial Proteins
  • Oligopeptides
  • Protein Sorting Signals
  • sortase E
  • Glutamine
  • Aminoacyltransferases
  • Transglutaminases
  • Cysteine Endopeptidases

Supplementary concepts

  • Streptomyces mobaraensis