Dual-Pharmacophore Pyrithione-Containing Cephalosporins Kill Both Replicating and Nonreplicating Mycobacterium tuberculosis

ACS Infect Dis. 2019 Aug 9;5(8):1433-1445. doi: 10.1021/acsinfecdis.9b00112. Epub 2019 Jun 11.

Abstract

The historical view of β-lactams as ineffective antimycobacterials has given way to growing interest in the activity of this class against Mycobacterium tuberculosis (Mtb) in the presence of a β-lactamase inhibitor. However, most antimycobacterial β-lactams kill Mtb only or best when the bacilli are replicating. Here, a screen of 1904 β-lactams led to the identification of cephalosporins substituted with a pyrithione moiety at C3' that are active against Mtb under both replicating and nonreplicating conditions, neither activity requiring a β-lactamase inhibitor. Studies showed that activity against nonreplicating Mtb required the in situ release of the pyrithione, independent of the known class A β-lactamase, BlaC. In contrast, replicating Mtb could be killed both by released pyrithione and by the parent β-lactam. Thus, the antimycobacterial activity of pyrithione-containing cephalosporins arises from two mechanisms that kill mycobacteria in different metabolic states.

Keywords: antimycobacterial; cephalosporin; pyrithione; tuberculosis; β-lactamase.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Administration, Oral
  • Animals
  • Antitubercular Agents / administration & dosage
  • Antitubercular Agents / pharmacology*
  • Callithrix
  • Cephalosporins / administration & dosage
  • Cephalosporins / pharmacology*
  • DNA Replication*
  • Drug Discovery
  • Female
  • Hep G2 Cells
  • High-Throughput Screening Assays
  • Humans
  • Mice
  • Mycobacterium tuberculosis / drug effects*
  • Mycobacterium tuberculosis / physiology
  • Pyridines / administration & dosage
  • Pyridines / pharmacology*
  • Thiones / administration & dosage
  • Thiones / pharmacology*

Substances

  • Antitubercular Agents
  • Cephalosporins
  • Pyridines
  • Thiones
  • pyrithione