Electrospraying Oxygen-Generating Microparticles for Tissue Engineering Applications

Int J Nanomedicine. 2020 Feb 19:15:1173-1186. doi: 10.2147/IJN.S237334. eCollection 2020.

Abstract

Background: The facile preparation of oxygen-generating microparticles (M) consisting of Polycaprolactone (PCL), Pluronic F-127, and calcium peroxide (CPO) (PCL-F-CPO-M) fabricated through an electrospraying process is disclosed. The biological study confirmed the positive impact from the oxygen-generating microparticles on the cell growth with high viability. The presented technology could work as a prominent tool for various tissue engineering and biomedical applications.

Methods: The oxygen-generated microparticles fabricated through electrospraying processes were thoroughly characterization through various methods such as X-ray diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR) analysis, and scanning electron microscopy (SEM)/SEM-Energy Dispersive Spectroscopy (EDS) analysis.

Results: The analyses confirmed the presence of the various components and the porous structure of the microparticles. Spherical shape with spongy characteristic microparticles were obtained with negative charge surface (ζ = -16.9) and a size of 17.00 ± 0.34 μm. Furthermore, the biological study performed on rat chondrocytes demonstrated good cell viability and the positive impact of increasing the amount of CPO in the PCL-F-CPO-M.

Conclusion: This technological platform could work as an important tool for tissue engineering due to the ability of the microparticles to release oxygen in a sustained manner for up to 7 days with high cell viability.

Keywords: calcium peroxide; cartilage; electrospraying; oxygen-generating-microparticles; tissue engineering.

MeSH terms

  • Animals
  • Biocompatible Materials / chemistry
  • Cell Culture Techniques
  • Cell Proliferation
  • Cell Survival / drug effects
  • Chondrocytes / drug effects
  • Electrochemical Techniques
  • Oxygen / chemistry
  • Oxygen / pharmacokinetics*
  • Peroxides / chemistry
  • Poloxamer / chemistry
  • Polyesters / chemistry
  • Porosity
  • Rats, Wistar
  • Spectrometry, X-Ray Emission
  • Spectroscopy, Fourier Transform Infrared
  • Tissue Engineering / methods
  • X-Ray Diffraction

Substances

  • Biocompatible Materials
  • Peroxides
  • Polyesters
  • Poloxamer
  • polycaprolactone
  • calcium peroxide
  • Oxygen