The Pimpled Gold Nanosphere: A Superior Candidate for Plasmonic Photothermal Therapy

Int J Nanomedicine. 2020 Apr 24:15:2903-2920. doi: 10.2147/IJN.S248327. eCollection 2020.

Abstract

Background: The development of highly efficient nanoparticles to convert light to heat for anti-cancer applications is quite a challenging field of research.

Methods: In this study, we synthesized unique pimpled gold nanospheres (PGNSs) for plasmonic photothermal therapy (PPTT). The light-to-heat conversion capability of PGNSs and PPTT damage at the cellular level were investigated using a tissue phantom model. The ability of PGNSs to induce robust cellular damage was studied during cytotoxicity tests on colorectal adenocarcinoma (DLD-1) and fibroblast cell lines. Further, a numerical model of plasmonic (COMSOL Multiphysics) properties was used with the PPTT experimental assays.

Results: A low cytotoxic effect of thiolated polyethylene glycol (SH-PEG400-SH-) was observed which improved the biocompatibility of PGNSs to maintain 89.4% cell viability during cytometry assays (in terms of fibroblast cells for 24 hrs at a concentration of 300 µg/mL). The heat generated from the nanoparticle-mediated phantom models resulted in ΔT=30°C, ΔT=23.1°C and ΔT=21°C for the PGNSs, AuNRs, and AuNPs, respectively (at a 300 µg/mL concentration and for 325 sec). For the in vitro assays of PPTT on cancer cells, the PGNS group induced a 68.78% lethality (apoptosis) on DLD-1 cells. Fluorescence microscopy results showed the destruction of cell membranes and nuclei for the PPTT group. Experiments further revealed a penetration depth of sufficient PPTT damage in a physical tumor model after hematoxylin and eosin (H&E) staining through pathological studies (at depths of 2, 3 and 4 cm). Severe structural damages were observed in the tissue model through an 808-nm laser exposed to the PGNSs.

Conclusion: Collectively, such results show much promise for the use of the present PGNSs and photothermal therapy for numerous anti-cancer applications.

Keywords: colorectal cells; gold nanoparticles; pathology; photothermal therapy; plasmonic.

MeSH terms

  • Adenocarcinoma / pathology
  • Adenocarcinoma / therapy
  • Apoptosis / drug effects
  • Cell Line, Tumor
  • Cell Survival / drug effects
  • Colorectal Neoplasms / pathology
  • Colorectal Neoplasms / therapy
  • Fibroblasts
  • Gold / chemistry
  • Humans
  • Lasers
  • Nanospheres / chemistry*
  • Nanospheres / therapeutic use*
  • Neoplasms / therapy
  • Phantoms, Imaging
  • Phototherapy / methods*
  • Polyethylene Glycols / chemistry

Substances

  • Polyethylene Glycols
  • Gold
  • polyethylene glycol 400