Identification of a PGXPP degron motif in dishevelled and structural basis for its binding to the E3 ligase KLHL12

Open Biol. 2020 Jun;10(6):200041. doi: 10.1098/rsob.200041. Epub 2020 Jun 24.

Abstract

Wnt signalling is dependent on dishevelled proteins (DVL1-3), which assemble an intracellular Wnt signalosome at the plasma membrane. The levels of DVL1-3 are regulated by multiple Cullin-RING E3 ligases that mediate their ubiquitination and degradation. The BTB-Kelch protein KLHL12 was the first E3 ubiquitin ligase to be identified for DVL1-3, but the molecular mechanisms determining its substrate interactions have remained unknown. Here, we mapped the interaction of DVL1-3 to a 'PGXPP' motif that is conserved in other known partners and substrates of KLHL12, including PLEKHA4, PEF1, SEC31 and DRD4. To determine the binding mechanism, we solved a 2.4 Å crystal structure of the Kelch domain of KLHL12 in complex with a DVL1 peptide that bound with low micromolar affinity. The DVL1 substrate adopted a U-shaped turn conformation that enabled hydrophobic interactions with all six blades of the Kelch domain β-propeller. In cells, the mutation or deletion of this motif reduced the binding and ubiquitination of DVL1 and increased its stability confirming this sequence as a degron motif for KLHL12 recruitment. These results define the molecular mechanisms determining DVL regulation by KLHL12 and establish the KLHL12 Kelch domain as a new protein interaction module for a novel proline-rich motif.

Keywords: BTB domain; Cul3; E3 ligase; Kelch; degradation; ubiquitin.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adaptor Proteins, Signal Transducing / chemistry*
  • Adaptor Proteins, Signal Transducing / genetics
  • Adaptor Proteins, Signal Transducing / metabolism*
  • Amino Acid Motifs
  • Binding Sites
  • Crystallography, X-Ray
  • Dishevelled Proteins / metabolism*
  • HEK293 Cells
  • Humans
  • Hydrophobic and Hydrophilic Interactions
  • Models, Molecular
  • Mutation*
  • Protein Binding
  • Protein Conformation
  • Protein Domains
  • Protein Stability
  • Ubiquitination
  • Wnt Signaling Pathway

Substances

  • Adaptor Proteins, Signal Transducing
  • DVL1 protein, human
  • Dishevelled Proteins
  • KLHL12 protein, human