Analytical validation of an error-corrected ultra-sensitive ctDNA next-generation sequencing assay

Biotechniques. 2020 Aug;69(2):133-140. doi: 10.2144/btn-2020-0045. Epub 2020 Jul 13.

Abstract

Plasma circulating tumor DNA (ctDNA) analysis has emerged as a minimally invasive means to perform molecular tumor typing. Here we developed a custom ultra-sensitive ctDNA next-generation sequencing assay using molecular barcoding technology and off-the-shelf reagents combined with bioinformatics tools for enhanced ctDNA analysis. Assay performance was assessed via a spike-in experiment and the technique was applied to analyze 41 plasma samples from men with advanced prostate cancer. Orthogonal validation was performed using a commercial assay. Sensitivity and specificity of 93 and 99.5% were recorded for ultra-rare somatic variants (<1%), with high concordance observed between the in-house and commercial assays. The optimized protocol dramatically improved the efficiency of the assay and enabled the detection of low-frequency somatic variants from plasma cell-free DNA (cfDNA).

Keywords: cell-free DNA; cfDNA; circulating tumor DNA; ctDNA; liquid biopsy; molecular barcoding; next-generation sequencing.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cell-Free Nucleic Acids / blood
  • Circulating Tumor DNA / blood*
  • High-Throughput Nucleotide Sequencing* / methods
  • High-Throughput Nucleotide Sequencing* / standards
  • Humans
  • Liquid Biopsy / methods
  • Liquid Biopsy / standards
  • Male
  • Prostatic Neoplasms / blood
  • Prostatic Neoplasms / pathology
  • Sensitivity and Specificity
  • Sequence Analysis, DNA* / methods
  • Sequence Analysis, DNA* / standards

Substances

  • Cell-Free Nucleic Acids
  • Circulating Tumor DNA